sonochemical synthesis of a cobalt(ii) coordination polymer nano-structure with azo ligand: a new precursor for preparation pure phase of co3o4 nanostructure
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abstract
a new nano-sized cobalt(ii) coordination polymer, (col1).0.5dmf.1.5ch3oh(1); [h2l1 = 5-(4-carboxy phenyl azo) salicyilic acid] has been synthesized by a sonochemical method. the thermal stability of compound 1 was studied by thermo- gravimetric and differential thermal analyses. nano-structure of this coordination polymer was characterized by elemental analyses, ir spectroscopy, powder x-ray diffraction and scanning electron microscopy. nano-particles of co3o4 were obtained by calcination of compound 1 at 550°c. the co3o4 nano-particles were characterized by powder x-ray diffraction and scanning electron microscopy.
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Journal title:
journal of nanostructuresPublisher: university of kashan
ISSN 2251-7871
volume 3
issue 1 2013
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